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Carius Method For Halogen Estimation

Hardchemistry

In Carius method, 0.245 g of an organic compound yields 0.287 g of AgCl. The percentage of chlorine in the compound is approximately:

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About This Question

Subject
chemistry
Chapter
purification and characterisation of organic compounds
Topic
carius method for halogen estimation
Difficulty
Hard
Year
2025
Tags
Carius MethodHalogen EstimationPercentage Composition

Solution

Correct Answer:

29.0%

Moles of AgCl = 0.287/143.32 = 2.003 x 10^-3 mol. Each mole AgCl contains 1 mole Cl, so mass of Cl = 2.003 x 10^-3 x 35.45 = 0.0710 g. Percentage Cl = (0.0710/0.245) x 100 = 28.98%, approximately 29.0%. The value is consistent with expected stoichiometry and mass balance.

This hard difficulty chemistry question is from the chapter purification and characterisation of organic compounds, covering the topic of carius method for halogen estimation. It appeared in the 2025 exam.

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